I never removed the engine block drain plug and followed a similar path to Mr Morlock and yourself.
1. Remove plug from bottom of radiator and drain into a container so you and note the quantity.
2. Flush out with hose and then fill with water (tap or distilled/demineralised) and run engine with the radiator cap off until top hose is warm.
3. Switch off and drain.
4. Repeat 2. and 3. until what drains out is just water.
5. Fill with coolant (and distilled/demineralised water if required) noting how much has been put in and compare with what you got in 1.
6. Drain clean expansion bottle and fill between low and high mark with coolant.
7. Run engine with radiator cap off until top hose gets warm and add coolant as the level drops as it cools - may take an hour or so.
8. Replace cap and take it for a drive near home and get it up to temperature, go home and switch it off and wait until fully cooled down. Check/add coolant to radiator/expansion bottle. Have you put back the same amount that came out?
9. Monitor closely over the next few days.
10. Don't let pets (cats/dogs) anywhere near spilled coolant - they like the smell/taste and it will kill them.